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                                                                                                                                                                                             NANOCHEMICAL LABORATORY

Synthesis
a hyper polyhydroxylated
fullerenol
C60(OH)60 by direct hydroxylation
of Fullerene from suspensions of  Fullerene in water.

      

Scientific and Technical Centre "Nanocluster" (STC "Nanocluster") developed an alternative the synthesis of hydroxylation of Fullerene to a hyper polyhydroxylated fullerenol 60(OH)60 from suspensions of  Fullerene in water. Synthesis takes place in one stage and is only in the aqueous phase, without the use of any solvents, including benzene, toluene, ortho-xylene. Synthesis duration is 20-30 min. Conversion (degree of reaction) Fullerene in water-soluble derivatives is about 98-99%. Synthesized hyper fullerenol 60(OH)60 is a yellow solid product. The solubility of this fullerenol in water is 60-70 grams per liter. The color of the solution of this fullerenol in the water is yellow (see picture):


Solution of a hyper polyhydroxylated fullerenol 60(OH)60 in the water 1

              Mass spectrum of this fullerenol corresponds to the fullerenol 60(OH)60: Base Peaks 1739.9879 is equal to the molecular weight of fullerenol 60(OH)60 (M=1740).

Mass spectrum of the fullerenol C60(OH)60

       Synthesis of simple and technological.  It can be used for the synthesis of a hyper polyhydroxylated fullerenol  60(OH)60 on an industrial scale. Fullerene can be used with a low degree of cleaning (98-99%).
        According to data the EA (elemental analysis), synthesized fullerenol has gross-formula 60(OH)60*22.

Result of Elemental Analysis of hyper fullerenol

Element

Percentage (%)

Analytical

Method

Date

Remark

 

C

 

 

40.5972

 

40.6017

 

 

Flash EA

1112

 

 

12/12/2016

 

 

H

 

 

3.6098

 

3.6113

Hyper polyhydroxylated fullerenol 60(OH)60 can be used in:

Pharmaceutics and cosmetology
    Antiviral medicine without cytotoxicity;
    Antioxidants, comparable to fullerenes under their effectiveness;
    Wound and burn healing medicine.

Materials science
    Modifiers of polymers, resins, glues, paint-and-lacquer and other materials;
    Modifiers of materials on base of silicate binding agents, including concretes;
    Component of electrolytes for metal galvanic coatings;
    Component of ultra-hard composite materials with metal matrix.

Agroindustry plant cultivation and animal husbandry
    Plant growth stimulants;
    Antiviral and antimycotic agents;
    Preparations, which increase stability of crops by complex nonspecific action;
    Additives to fodders, which increase resistibility of agricultural animals and birds to different diseases, and which do not accumulate in their organ
ism.


STC "Nanocluster" offers:
Hyper polyhydroxylated fullerenol 60()60 - 195 - 395 $US per gram
Minimum  batch - 3g

Phone: +7 912 210 67 55
E-mail: 
alex.kozeev@yandex.ru  or   info@nanoclaster.ru
Web-site:
www.nanoclaster.ru